HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl chloroglyoxylate → HCID 42630377, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl chloroglyoxylate | HCID 79846 | — |
| Reactant | 6-(5-Methyl-3-phenyl-isoxazol-4-ylmethoxy)-pyridazin-3-ylamine | HCID 42629771 | — |
| Product | HCID 42630377 | HCID 42630377 | 44% |
Reaction Steps
As described for example 18, 6-(5-methyl-3-phenyl-isoxazol-4-ylmethoxy)-pyridazin-3-ylamine (200 mg, 0.7 mmol) was converted, using chloro-oxo-acetic acid methyl ester instead of methoxyacetyl chloride, to the title compound (88 mg, 44%) which was obtained as a white solid. MS: m/e=369.0 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07943619B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-1f1dcbdf2f2146f2b22b769b68127deb |
| Source note | uspto-grants-2011_05 |