HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropanemethanamine → HCID 42630131, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropanemethanamine | HCID 75646 | — |
| Reactant | HCID 42630252 | HCID 42630252 | — |
| Reactant | HCID 42630253 | HCID 42630253 | — |
| Product | HCID 42630131 | HCID 42630131 | 26% |
Reaction Steps
As described for example 50, 6-[3-(4-fluoro-phenyl)-5-methyl-isoxazol-4-ylmethoxy]-pyridazine-3-carboxylic acid ethyl ester (143 mg, 0.4 mmol), instead of 6-[3-(3-fluoro-phenyl)-5-methyl-isoxazol-4-ylmethoxy]-pyridazine-3-carboxylic acid ethyl ester, was converted, using aminomethylcyclopropane instead of methylamine, to the title compound (39 mg, 26%) which was obtained as a white solid. MS: m/e=383.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07943619B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-539f64d136ef40a385a8c0383b157bea |
| Source note | uspto-grants-2011_05 |