HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 42630625, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 67157617 | HCID 67157617 | — |
| Product | HCID 42630625 | HCID 42630625 | 17% |
Reaction Steps
As described for example 69, 6-(5-methyl-3-pyridin-4-yl-isoxazol-4-ylmethoxy)-pyridazine-3-carboxylic acid ethyl ester (100 mg, 0.29 mmol) was converted, using methylamine (2 M solution in THF) instead of isopropylamine, to the title compound (16 mg, 17%) which was obtained as a white solid. MS: m/e=326.1 [M+H]−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07943619B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-b236dbf951f744a4b193c354bef45809 |
| Source note | uspto-grants-2011_05 |