HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → 6-(s-Triazolo[4,3-a]pyridin-3-ylthio)hexylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 19956977 | HCID 19956977 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 6-(s-Triazolo[4,3-a]pyridin-3-ylthio)hexylamine | HCID 19956995 | 87.5% |
Reaction Steps
A mixture of N-[6-(s-triazolo[4,3-a]pyridin-3-ylthio)hexyl]phthalimide (16.5 g), hydrazine monohydrate (4.34 g) and ethanol (135 ml) was heated under reflux for 1 hour. The deposited crystals were separated by filtration, and the filtrate was concentrated under reduced pressure to obtain 6-(s-triazolo[4,3-a]pyridin-3-ylthio)hexylamine as an oil. Yield: 87.5%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05624917 |
| Source dataset | uspto-grants-1997_04 |
| ORD ID | ord-8dd4f6880f55484eb55f6522407ce1b0 |
| Source note | uspto-grants-1997_04 |