HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylmethanesulfonyl chloride → 1-Phenylmethanesulfonyl-4-piperazin-1-yl-1 H-pyrrolo[3,2-c]pyridine Hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylmethanesulfonyl chloride | HCID 74740 | — |
| Reactant | 1-Piperazinecarboxylic acid,4-(1h-pyrrolo[3,2-c]pyridin-4-yl)-,1,1-dimethylethyl ester | HCID 67156709 | — |
| Product | 1-Phenylmethanesulfonyl-4-piperazin-1-yl-1 H-pyrrolo[3,2-c]pyridine Hydrochloride | HCID 67157510 | — |
Reaction Steps
Phenyl-methanesulfonyl chloride (24.6 mg) was added to tert-butyl 4-(1H-pyrrolo[3,2-c]pyridin-4-yl)piperazine-1-carboxylate the title compound (0.2 mg). LC/MS RT: 1.007 (System 10 till 40% MeCN over 1.5 min, ACE C8), Purity. 90%. MS: 357 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07943639B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-7bec195fb1ab4e15bf6f7aecf9a587fe |
| Source note | uspto-grants-2011_05 |