HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 67151152, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 67151029 | HCID 67151029 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67151152 | HCID 67151152 | — |
Reaction Steps
A mixture of 3-bromo-6-methoxyphenanthrene-9,10-dione from Step 3 above and excess BBr3 in CH2Cl2 was stirred at room temperature to afford 3-bromo-6-hydroxyphenanthrene-9,10-dione which was used directly in the next step (Step 5 below).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07943649B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-9f62ba04dff34444b66b9400321fd723 |
| Source note | uspto-grants-2011_05 |