HRID549942

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID7172298

tert-Butyl 4-(4-formyl-1,3-thiazol-2-yl)piperidine-1-carboxylate

C14H20N2O3S

结构：CC(CC[P+](c1ccccc1)(c1ccccc1)c1ccccc1)c1ccccc1.[I-]

HCID86642044

未命名化合物

PRODUCTS

生成物

$结构：CC(C/C=C\c1csc(C2CCN(C(=O)OC(C)(C)C)CC2)n1)c1ccccc1$

HCID67157181

未命名化合物

PROCEDURE

实验过程

tert-Butyl 4-(4-formyl-1,3-thiazol-2-yl)piperidine-1-carboxylate (1.00 g) is reacted with triphenyl(3-phenylbutyl)phosphonium iodide (3.53 g) and purified as described in IV-3. This gives tert-butyl 4-{4-[(1Z)-4-phenylpent-1-en-1-yl]-1,3-thiazol-2-yl}piperidine-1-carboxylate (1.23 g) in form of the Z isomer.

WORKUP

后处理

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