Acrylic Acid → HCID 86616912, compound

HRID 550052Notes

Reaction equation

HRID 550052 reaction equation
[CH:1]([O-:4])([CH3:3])[CH3:2].[CH:5]([O-:8])([CH3:7])[CH3:6].C([O-])(C)C.[Al+3:13].[C:14]([OH:18])(=[O:17])[CH:15]=[CH2:16]>>[CH:1]([O-:4])([CH3:3])[CH3:2].[CH:5]([O-:8])([CH3:7])[CH3:6].[C:14]([O-:18])(=[O:17])[CH:15]=[CH2:16].[Al+3:13]

Participants

3

Reactant 2

HCID 6581Acrylic AcidHCID 11143Aluminum isopropoxide

Product 1

HCID 86616912HCID 86616912, compound

Conditions

Temperature
32 °C

Procedure

Into the flask described hereinabove there were placed 204.2 grams of aluminium tri-iso-propanolate to which 72 grams of acrylic acid were added during 8 minutes at room temperature (25° C.). The procedure was as set forth hereinabove. Owing to the reaction heat, the temperature increased to 32° C. The resultant product was a white, solid substance. The rotary evaporator heating then was switched on and gradually heated to 70° C. At the same time the vacuum was gradually adjusted to 24 mbar. The isopropanol was thereby expelled yielding a white powder.

Workup

  1. additionwere added during 8 minutes at room temperature (25° C.)
  2. temperatureOwing to the reaction heat
  3. customThe rotary evaporator
  4. temperatureheating
  5. temperaturegradually heated to 70° C
  6. customThe isopropanol was thereby expelled yielding a white powder

Sources & evidence

ORD record
ord-47d2d0ad549149249ece2c3710de0a2d
Source dataset
uspto-grants-2011_05
Patent number
US07943798B2

Reaction notes

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