Acrylic Acid → HCID 86616912, compound

Participants

Reaction Conditions

Reaction Steps

Into the flask described hereinabove there were placed 204.2 grams of aluminium tri-iso-propanolate to which 72 grams of acrylic acid were added during 8 minutes at room temperature (25° C.). The procedure was as set forth hereinabove. Owing to the reaction heat, the temperature increased to 32° C. The resultant product was a white, solid substance. The rotary evaporator heating then was switched on and gradually heated to 70° C. At the same time the vacuum was gradually adjusted to 24 mbar. The isopropanol was thereby expelled yielding a white powder.

Provenance & Evidence