HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 66631059, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 11463864 | HCID 11463864 | — |
| Product | HCID 66631059 | HCID 66631059 | — |
Reaction Steps
Using an analogous procedure to that described in Example 36, N-cyclopropyl-4-methyl-3-({4-[(5-methylisoxazol-3-yl)methoxy]benzoyl}amino)benzamide was reacted with hydrobromic acid to give the title compound; NMR Spectrum: (DMSOd6) 0.57 (m, 2H), 0.68 (m, 2H), 2.26 (s, 3H), 2.44 (5, 3H), 2.85 (m, 1H), 5.25 (s, 2H), 6.37 (s, 1H), 7.15 (m, 2H), 7.31 (m, 1H), 7.61 (m, 1H), 7.78 (s, 1H), 7.98 (m, 2H), 8.37 (s, 1H), 9.82 (s, 1H); Mass Spectrum: M−H− 404, M+Na+ 428.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07943776B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-690daceb8e9849d68ed9d797008866fb |
| Source note | uspto-grants-2011_05 |