HRID550383

反应详情

EQUATION

反应方程式

HRID 550383 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

tert-Butyl 4-{[2-(2-nitrophenyl)ethyl]amino}piperidine-1-carboxylate and 10% palladium on carbon (1.9 g) were stirred in ethanol (250 mL) overnight under one atmosphere hydrogen. Catalyst was filtered from the solution and solvent removed in vacuo to provide the title compound (17.2 g). MS: m/z=320 (M+1)

WORKUP

后处理

  1. filtrationCatalyst was filtered from the solution and solvent
  2. customremoved in vacuo