HRID550529

反应详情

EQUATION

反应方程式

HRID 550529 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of methyl 4-pyridazinecarboxylate (400 mg, 2.9 mmol) in MeOH (5 ml) was added hydrazine monohydrate (23 mmol). The solution was heated to reflux for 12 h. Volatiles were evaporated in vacuo to give 395 mg of the title compound as a yellow pale foam, which was used without further purification.

WORKUP

后处理

  1. temperatureThe solution was heated
  2. temperatureto reflux for 12 h
  3. customVolatiles were evaporated in vacuo