HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dimethylthiazole-5-carbohydrazide → 3-(2,4-dimethyl-1,3-thiazol-5-yl)-4-methyl-5-(4-penten-1-yl)-4H-1,2,4-triazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dimethylthiazole-5-carbohydrazide | HCID 2743669 | — |
| Reactant | N,N'-dimethyl-5-hexenimidamide hydrochloride | HCID 86630240 | — |
| Product | 3-(2,4-dimethyl-1,3-thiazol-5-yl)-4-methyl-5-(4-penten-1-yl)-4H-1,2,4-triazole | HCID 57691947 | — |
Reaction Steps
The title compound was prepared in analogy to Preparation 11 in 0.17 g yield starting from 2,4-dimethyl-1,3-thiazole-5-carbohydrazide (0.50 g) and N,N′-dimethyl-5-hexenimidamide hydrochloride (0.51 g). MS (m/z): 263 [MH]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07947683B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-82e1d6ae89a7460dada36acc64d5fcaf |
| Source note | uspto-grants-2011_05 |