Sodium triacetoxyborohydride → HCID 59663073, compound

HRID 550639Notes

Reaction equation

[CH3:1][C:2]1[C:6]2[C:7]([CH3:11])=[N:8][CH2:9][CH2:10][C:5]=2[S:4][CH:3]=1.C(O[BH-](OC(=O)C)OC(=O)C)(=O)C.[Na+]>>[CH3:1][C:2]1[C:6]2[CH:7]([CH3:11])[NH:8][CH2:9][CH2:10][C:5]=2[S:4][CH:3]=1

Participants

Reactant 2

HCID 5049666Sodium triacetoxyborohydride

HCID 59663081HCID 59663081, compound

Product 1

HCID 59663073HCID 59663073, compoundYield 8%

Procedure

In close analogy to the procedure described above, 3,4-Dimethyl-6,7-dihydro-thieno[3,2-c]pyridine is reacted with sodium triacetoxyborohydride to provide the title compound.

Sources & evidence

ORD record: ord-4d8eac2eb56540cf882bd491457207b8
Source dataset: uspto-grants-2011_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07947689B2

Reaction notes

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