HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromomethyl-1,4-benzodioxane → HCID 67200928, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromomethyl-1,4-benzodioxane | HCID 98333 | — |
| Reactant | HCID 67200730 | HCID 67200730 | — |
| Product | HCID 67200928 | HCID 67200928 | — |
Reaction Steps
3-Allyloxy-1-(3-bromo-benzyl)-1H-thieno[3,2-d]pyrimidine-2,4-dione was alkylated with 2-bromomethyl-2,3-dihydro-benzo[1,4]dioxine via general procedure B2. The crude intermediate was deprotected via general procedure D2. The final product was purified by mass triggered preparative HPLC. Electrospray MS: 333 (M+H); retention time: 2.05 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07947691B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-8ff2a863543a44719583ab6d7ddf1529 |
| Source note | uspto-grants-2011_05 |