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HRID550716

反应详情

EQUATION

反应方程式

HRID 550716 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)c1cccc(B(O)O)c1
HCID2734310

3-Acetylphenylboronic acid

C8H9BO3

结构：O=c1c2sccc2n(Cc2cccc(Br)c2)c(=O)n1O
HCID11544874

1-[(3-Bromophenyl)methyl]-3-hydroxythieno[3,2-d]pyrimidine-2,4(1H,3H)-dione

C13H9BrN2O3S

PRODUCTS

生成物

1
结构：CC(=O)c1cccc(-c2cccc(Cn3c(=O)n(O)c(=O)c4sccc43)c2)c1
HCID11625324

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 1-(3-Bromo-benzyl)-3-hydroxy-1H-thieno[3,2-d]pyrimidine-2,4-dione (from previous example) and 3-acetyl-phenyl boronic acid via general procedure C. The crude product was purified by mass-triggered preparative HPLC.

WORKUP

后处理

  1. customThe crude product was purified by mass-triggered preparative HPLC