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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 550731Generated: October 31, 2026

Picolyl chloride hydrochloride → HCID 11666995, compound

https://huagongshe.com/reaction/550731

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPicolyl chloride hydrochlorideHCID 23392—
Reactant3-(2,4-Dimethoxy-benzyloxy)-1H-benzo[4,5]thieno[3,2-d]pyrimidine-2,4-dioneHCID 67200934—
ProductHCID 11666995HCID 11666995—

Reaction Steps

Following general procedure B2 and D1, 3-(2,4-Dimethoxy-benzyloxy)-1H-benzo[4,5]thieno[3,2-d]pyrimidine-2,4-dione was alkylated with 2-chloromethylpyridine hydrochloride and subsequently deprotected to provide the title compound as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07947691B2
Source datasetuspto-grants-2011_05
ORD IDord-4dc1c224f0834efdafca1242df6e226b
Source noteuspto-grants-2011_05