HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloride → HCID 59257860, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloride | HCID 312 | — |
| Reactant | HCID 86629735 | HCID 86629735 | — |
| Product | HCID 59257860 | HCID 59257860 | — |
Reaction Steps
Essentially following the procedures described for Intermediate 34, but using (±)-ethyl 3-[1-(2-tert-butoxy-2-oxoethyl)-4-nitro-2,3-dihydro-1H-indol-3-yl]propanoate in place of ethyl 3-[1-(2-tert-butoxy-2-oxoethyl)-4-nitro-1H-indol-3-yl]propanoate, and resolving the racemate into pure enantiomers in analogy with Intermediate 42, the title compound was prepared. MS: m/z=303 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07947677B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-2c741f6ca93c461da4f7bf9a03393763 |
| Source note | uspto-grants-2011_05 |