Hydrochloric Acid → HCID 178499561, compound

HRID 55109Notes

Reaction equation

HRID 55109 reaction equation
[ClH:1].[NH:2]1[CH:6]=[C:5]([CH2:7][C:8]([OH:10])=[O:9])[N:4]=[CH:3]1.Cl.[CH3:12]O>>[ClH:1].[CH3:12][O:9][C:8](=[O:10])[CH2:7][C:5]1[N:4]=[CH:3][NH:2][CH:6]=1

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 887MethanolHCID 178479752HCID 178479752, compound

Product 1

HCID 178499561HCID 178499561, compound

Procedure

A solution of 1H-imidazole-4-acetic acid hydrochloride (4.00 g, 24.6 mmol) in methanol (100 ml) was saturated with gaseous hydrogen chloride. The resulting solution was allowed to stand at room temperature (RT) for 18 hr. The solvent was evaporated in vacuo to afford the title compound as a white solid.

Workup

  1. customto stand at room temperature
  2. custom(RT)
  3. customfor 18 hr
  4. customThe solvent was evaporated in vacuo

Sources & evidence

ORD record
ord-a6718c34031b48c99f1c7485688f68e9
Source dataset
uspto-grants-1997_04
Patent number
US05624936

Reaction notes

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