HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67188417, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 24852911 | HCID 24852911 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 67188417 | HCID 67188417 | — |
Reaction Steps
5.82 ml of a 0.2N solution of hydrochloric acid in ether are added to a 25 ml round-bottomed flask comprising 0.18 g of 4-[(3-(pyridin-3-yl)pyrrolidin-1-yl)carbonyl]-3,4-dihydro-2H-1,4-benzoxazine. Stirring is maintained for 10 min. After evaporating, the residue is taken up in ether. The precipitate is filtered off and then dried under vacuum. 0.12 g of 4-[(3-(pyridin-3-yl)pyrrolidin-1-yl)carbonyl]-3,4-dihydro-2H-1,4-benzoxazine hydrochloride is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07947834B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-ff1a26fc292f4d919b57d9664e0fbc0b |
| Source note | uspto-grants-2011_05 |