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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 551788Generated: November 2, 2026

Hydrochloric Acid → HCID 67188417, compound

https://huagongshe.com/reaction/551788

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 24852911HCID 24852911—
SolventDiethyl EtherHCID 3283—
ProductHCID 67188417HCID 67188417—

Reaction Steps

5.82 ml of a 0.2N solution of hydrochloric acid in ether are added to a 25 ml round-bottomed flask comprising 0.18 g of 4-[(3-(pyridin-3-yl)pyrrolidin-1-yl)carbonyl]-3,4-dihydro-2H-1,4-benzoxazine. Stirring is maintained for 10 min. After evaporating, the residue is taken up in ether. The precipitate is filtered off and then dried under vacuum. 0.12 g of 4-[(3-(pyridin-3-yl)pyrrolidin-1-yl)carbonyl]-3,4-dihydro-2H-1,4-benzoxazine hydrochloride is obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07947834B2
Source datasetuspto-grants-2011_05
ORD IDord-ff1a26fc292f4d919b57d9664e0fbc0b
Source noteuspto-grants-2011_05