HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 10870927, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 11141634 | HCID 11141634 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 10870927 | HCID 10870927 | — |
Reaction Steps
24 was prepared by reduction of 3β-methoxyandrost-5-ene-7,17-dione 20, with sodium borohydride in a mixture of methylene dichloride-methanol at room temperature. The product was purified by column chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07947846B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-51a5c272897e4d1e8591c91778a0121e |
| Source note | uspto-grants-2011_05 |