反应详情

To a stirred solution of 6-(6-dibenzylamino-3-azabicyclo[3.1.0]hex-3-yl)pyridazine-3-carboxylic acid (2-cyclopropylethyl)amide (0.415 g, 0.90 mmol) in methanol (10 mL) was added Pd/C (0.200 g, 12 mol %). The mixture was placed under an atmosphere of hydrogen for 3 days. The reaction mixture was filtered through celite and concentrated in vacuo. The crude title compound was obtained and used without further purification.

1. filtrationThe reaction mixture was filtered through celite and
2. concentrationconcentrated in vacuo