HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67170729, compound → HCID 67172284, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67170729 | HCID 67170729 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67172284 | HCID 67172284 | — |
Reaction Steps
To a stirred solution of 6-(6-dibenzylamino-3-azabicyclo[3.1.0]hex-3-yl)pyridazine-3-carboxylic acid (2-cyclopropylethyl)amide (0.415 g, 0.90 mmol) in methanol (10 mL) was added Pd/C (0.200 g, 12 mol %). The mixture was placed under an atmosphere of hydrogen for 3 days. The reaction mixture was filtered through celite and concentrated in vacuo. The crude title compound was obtained and used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07951805B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-ff5b104bfff04e5ca4ecf94e9caa3c7e |
| Source note | uspto-grants-2011_05 |