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HRID552180

反应详情

EQUATION

反应方程式

HRID 552180 的结构方程式

REACTANTS

反应物

2
结构：Cc1ncccc1C(=O)O
HCID643373

2-methylnicotinic acid

C7H7NO2

结构：CCOc1c(Cl)cc2c([nH]c3cnccc32)c1N
HCID67164452

未命名化合物

PRODUCTS

生成物

1
结构：CCOc1c(Cl)cc2c([nH]c3cnccc32)c1NC(=O)c1cccnc1C
HCID11440410

未命名化合物

收率 40%

PROCEDURE

实验过程

The desired compound was prepared according to Method A from 6-chloro-7-ethoxy-9H-β-carbolin-8-ylamine and 2-methylnicotinic acid in 40% yield. 1H-NMR (300 MHz, MeOH-d4): δ 1.39 (t, 3H), 2.76 (s, 3H), 4.14 (q, 2H), 7.43 (dd, 1H), 8.05 (d, 1H), 8.26 (m, 3H), 8.55 (d, 1H), 8.79 (s, 1H).