HCID 9031607, compound → HCID 57424172, compound

Participants

Reaction Steps

To a solution of N-(4-dimethylamino-benzyl)-4-nitro-benzenesulfonamide (472 mg, 1.409 mmol), prepared as described in D.1, in MeOH (10 ml) under nitrogen was added Pd/C 10% (74.92 mg, 0.007 mmol). The system was purged with hydrogen and let stirred overnight under an atmosphere of hydrogen. After filtration through a celite plug, the solvent is removed under reduced pressure to yield the title compound, which is used as such for the next step.

Provenance & Evidence