HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl triflate → HCID 73446474, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl triflate | HCID 9526 | — |
| Reactant | HCID 72741676 | HCID 72741676 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 73446474 | HCID 73446474 | — |
Reaction Steps
17.4 ml (120 mmol) of methyl trifluoromethanesulfonate are added dropwise at 0° C. to a suspension of 35 g (120 mmol) of phenyl(pyridin-2-yl)methanone O-benzyloxime in 200 ml of diethyl ether, and the mixture is stirred at room temperature for 3 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07951821B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-e86884a91168423b9f603378842eeea7 |
| Source note | uspto-grants-2011_05 |