huagongshe.com
HRID552509

反应详情

EQUATION

反应方程式

HRID 552509 的结构方程式

REACTANTS

反应物

2
结构：Cc1cc(Br)ccn1
HCID2762835

4-Bromo-2-methylpyridine

C6H6BrN

结构：Cc1cc(NC(=O)c2cc(B3OC(C)(C)C(C)(C)O3)cc(C)n2)ccn1
HCID67164968

6-Methyl-N-(2-methyl-4-pyridinyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2-pyridinecarboxamide

C19H24BN3O3

PRODUCTS

生成物

1
结构：Cc1cc(NC(=O)c2cc(-c3ccnc(C)c3)cc(C)n2)ccn1
HCID67163295

未命名化合物

PROCEDURE

实验过程

The title compound, was prepared from 6-Methyl-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-pyridine-2-carboxylic acid (2-methyl-pyridin-4-yl)-amide in accordance with the general method of example 131, step 2 using 4-Bromo-2-methylpyridine instead of 3-Trifluoromethyl-5-bromopyridine to yield the final compound as a colorless amorphous, MS (ISP): m/e=319.2 (M+H)+.