HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2-methylpyridine → HCID 67163295, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2-methylpyridine | HCID 2762835 | — |
| Reactant | 6-Methyl-N-(2-Methylpyridin-4-yl)-4-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)picolinaMide | HCID 67164968 | — |
| Product | HCID 67163295 | HCID 67163295 | — |
Reaction Steps
The title compound, was prepared from 6-Methyl-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-pyridine-2-carboxylic acid (2-methyl-pyridin-4-yl)-amide in accordance with the general method of example 131, step 2 using 4-Bromo-2-methylpyridine instead of 3-Trifluoromethyl-5-bromopyridine to yield the final compound as a colorless amorphous, MS (ISP): m/e=319.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07951824B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-2c33fe67d7b94d0fa2bc47b5784adc02 |
| Source note | uspto-grants-2011_05 |