HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → 5-Fluoro-6'-methyl-[3,4']bipyridinyl-2'-carboxylic acid phenylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 5-Fluoro-6'-methyl-[3,4']bipyridinyl-2'-carboxylic acid ethyl ester | HCID 67164770 | — |
| Product | 5-Fluoro-6'-methyl-[3,4']bipyridinyl-2'-carboxylic acid phenylamide | HCID 67162954 | — |
Reaction Steps
The title compound, was prepared from 5-Fluoro-6′-methyl-[3,4′]bipyridinyl-2′-carboxylic acid ethyl ester in accordance with the general method of example 26, step 6 using Aniline instead of 3-chloroaniline to yield the final compound as a white solid, MS (ISP): m/e=308.3, 309.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07951824B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-cf726e268d404d85bd70362fb4cb4b46 |
| Source note | uspto-grants-2011_05 |