HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 67165528, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 24820980 | HCID 24820980 | — |
| Product | HCID 67165528 | HCID 67165528 | — |
Reaction Steps
The title compound, was prepared by treatment of 4-(3,5-Difluorophenyl)-6-methyl-pyridine-2-carboxylic acid (1-carbamoylmethyl-1H-pyrazol-3-yl)-amide with POCl3 in accordance with the general method of example 163, step 2 to yield the final compound as a white solid, MS (ISP): m/e=354.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07951824B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-7961b904f64747d286c090e2be4cb0f2 |
| Source note | uspto-grants-2011_05 |