HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium methanesulfinate → 4-(3-Methanesulfonyl-propoxy)-benzoic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium methanesulfinate | HCID 2733271 | — |
| Reactant | Methyl 4-(3-bromopropoxy)benzoate | HCID 3709742 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 4-(3-Methanesulfonyl-propoxy)-benzoic acid methyl ester | HCID 59786770 | — |
Reaction Steps
The title compound is prepared in a manner substantially analogous to Procedure C starting from 4-(3-bromo-propoxy)-benzoic acid methyl ester and methanesulfinic acid sodium salt using DMF as solvent. MS (ES+) 273.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07951826B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-66209c1ee8e64b1b83ec6242d9ba51af |
| Source note | uspto-grants-2011_05 |