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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 552714Generated: November 2, 2026

Diisopropylethylamine → HCID 178478406, compound

https://huagongshe.com/reaction/552714

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiisopropylethylamineHCID 81531—
Reactant2,6-DichloropurineHCID 5324412—
Reactant1-Aminoindane, (S)-HCID 7000084—
SolventEthanolHCID 702—
ProductHCID 178478406HCID 17847840680%

Reaction Steps

(S)-(+)-1-Aminoindane (266.0 mg, 2.0 mmol), 2,6-dichloropurine (380 mg, 2.0 mmol) and N,N-diisopropylethylamine (380 μL, 2.2 mmol), were dissolved in Ethanol (4.0 mL) and reacted in a microwave at 120° C. for 600 s. A yellow solid formed which was filtered, washed with ethanol (20 mL) and dried to give the title compound 0.455 g, 80% yield.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07951810B2
Source datasetuspto-grants-2011_05
ORD IDord-66a5b82ee7ad45e3aae907941fd0369b
Source noteuspto-grants-2011_05