HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → Methyl 6-iodo-5-methoxypicolinate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 6-Iodo-5-methoxypyridine-2-carboxylic acid | HCID 7471968 | — |
| Product | Methyl 6-iodo-5-methoxypicolinate | HCID 49766559 | — |
Reaction Steps
Under the conditions of example 1 D, 9.8 g of 2-iodo-3-methoxy-pyridine-6-carboxylic acid is reacted with 2.5 ml of iodomethane and worked up. 7.4 g of 2-iodo-3-methoxypyridine-6-carboxylic acid methyl ester of melting point 175°-178° C. is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05624943 |
| Source dataset | uspto-grants-1997_04 |
| ORD ID | ord-569eeecdaff24d0eab83b6f7d8337f66 |
| Source note | uspto-grants-1997_04 |