HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54542739, compound → 3-(6-Carboxy-3-hydroxy-2-pyridyl)-propionic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54542739 | HCID 54542739 | — |
| Solvent | Hydrogen Bromide | HCID 260 | — |
| Product | 3-(6-Carboxy-3-hydroxy-2-pyridyl)-propionic acid | HCID 19957489 | 75.6% |
Reaction Steps
Under the conditions of example 16K, 6.5 g of 3-(3-methoxy-6-methoxycarbonyl-2-pyridyl)-propionic acid methyl ester in 60 ml of 48% hydrobromic acid is reacted and worked up. 4.1 g of 3-(6-carboxy-3-hydroxy-2-pyridyl)-propionic acid of melting point 210°-212° C. is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05624943 |
| Source dataset | uspto-grants-1997_04 |
| ORD ID | ord-7be800e0f7bb4867a4b32027d58d7214 |
| Source note | uspto-grants-1997_04 |