HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → Methyl 2-(3-bromophenyl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | (3-Bromophenyl)acetic acid | HCID 74653 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl 2-(3-bromophenyl)acetate | HCID 11746402 | — |
Reaction Steps
Acetyl chloride (5 mL) was added to a solution of (3-bromo-phenyl)-acetic acid (10 g) in methanol (250 mL). Evaporation after 24 hours afforded the subtitle product, as an oil (10.9 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07951954B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-e87e49a88e694d5ba7254c3cfa76baa7 |
| Source note | uspto-grants-2011_05 |