HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 86612199, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Thioanisole | HCID 7520 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86612199 | HCID 86612199 | — |
Reaction Steps
At room temperature, 6.2 g (0.05 mole) of thioanisole and 6.9 g (0.055 mole) of dimethyl sulfate were stirred for 12 hours. To the reaction solution were added 100 g of water and 50 ml of diethyl ether. The water layer was taken out, obtaining an aqueous solution of the desired dimethylphenylsulfonium sulfate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048610B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-af305775d42441828db19ac705114b02 |
| Source note | uspto-grants-2011_11 |