HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzathine → HCID 67462775, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzathine | HCID 8793 | — |
| Reactant | Cyanogen Bromide | HCID 10476 | — |
| Product | HCID 67462775 | HCID 67462775 | — |
Reaction Steps
The title compound was prepared in one step from N,N′-dibenzylethylenediamine and cyanogen bromide as described in Procedure A. The precipitated solid was filtered off the reaction mixture, washed with acetonitrile and recrystallized from MeOH to give the title compound as a hydrogen bromide salt. 1NMR (DMSO-d6) δ 3.48 (s, 4H), 4.61 (s, 4H), 7.32-7.46 (m, 10H), 8.51 (s, 2H). MS (ES+) m/z 266 ([M+1]+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048877B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-d31747627a3345cbaa03bda352f83eeb |
| Source note | uspto-grants-2011_11 |