HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 44596878, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 44596874 | HCID 44596874 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 44596878 | HCID 44596878 | — |
Reaction Steps
Triethylamine (303 mg, 3 mmol) and 10% Pd—C (20 mg) were added to Compound 2.7 (500 mg, 1.05 mmol) in MeOH (5 mL) and the mixture was hydrogenated on a Parr shaker at 40 PSI for 90 min. The mixture was filtered through Celite and concentrated. The product was used in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048895B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-b7a03a23ac1d482f9a471ec582f4aadc |
| Source note | uspto-grants-2011_11 |