Ethyl Acetoacetate → HCID 178429290, compound

Participants

Reaction Steps

Benzamidine hydrochloride (1.56 g), ethyl acetoacetate (1.26 ml) and sodium methoxide (30% in MeOH, 3.7 ml) were dissolved in EtOH (10 ml) and the resulting mixture was refluxed overnight. It was cooled down and the white suspension was filtered off. The solid was washed with water and high-vacuum dried. 1.83 g of a white solid were obtained.

Provenance & Evidence