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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 553876Generated: October 30, 2026

Triethyl phosphite → HCID 86612696, compound

https://huagongshe.com/reaction/553876

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethyl phosphiteHCID 31215—
ReactantHCID 69077078HCID 69077078—
ProductHCID 86612696HCID 86612696—

Reaction Conditions

Temperature120 °C

Reaction Steps

A mixture of (5S*,8aR*)-5-(4-fluorophenyl)-2-iodohexahydroindolizin-3-one (120 mg) with triethyl phosphite (2 mL) was stirred at 120° C. for 14 hours. The reaction solution was left to cool to room temperature and then concentrated under reduced pressure to obtain 123 mg of the title compound. The property value of the compound is as follows.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08048878B2
Source datasetuspto-grants-2011_11
ORD IDord-b3839a51533148958edb713d6932f2c3
Source noteuspto-grants-2011_11