HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Acetate → HCID 66924664, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Reactant | HCID 66924672 | HCID 66924672 | — |
| Product | HCID 66924664 | HCID 66924664 | 96.3% |
Reaction Steps
Using ethyl 2-acetyl-3-methyl-4-oxo-4-(3-thienyl)butanoate (1.86 g) and ammonium acetate (626 mg), a procedure as in Reference Example 14 was performed to give the title compound as a brown oil (yield 1.57 g, 91%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048909B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-ffa2e79740bb4803b23ad0b06a460de7 |
| Source note | uspto-grants-2011_11 |