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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 554289Generated: October 29, 2026

Diisobutylaluminumhydride → HCID 66924627, compound

https://huagongshe.com/reaction/554289

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiisobutylaluminumhydrideHCID 21225700—
ReactantHCID 66925021HCID 66925021—
SolventTolueneHCID 1140—
ProductHCID 66924627HCID 6692462763%

Reaction Steps

Using methyl 2-methyl-1-(phenylsulfonyl)-5-(3-thienyl)-1H-pyrrole-3-carboxylate (0.75 g) and a 1.5 mol/L solution (4.0 mL) of diisobutylaluminum hydride in toluene, a procedure as in Reference Example 5 was performed to give the title compound as a brown oil (yield 0.42 g, 63%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08048909B2
Source datasetuspto-grants-2011_11
ORD IDord-50e7336468cf4fed9bcefc20c3ff260a
Source noteuspto-grants-2011_11