Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 554291Generated: October 31, 2026

Diisobutylaluminumhydride → HCID 66924715, compound

https://huagongshe.com/reaction/554291

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiisobutylaluminumhydrideHCID 21225700—
ReactantHCID 66924705HCID 66924705—
SolventTolueneHCID 1140—
ProductHCID 66924715HCID 6692471594%

Reaction Steps

Using ethyl 2,4-dimethyl-5-phenyl-1-(phenylsulfonyl)-1H-pyrrole-3-carboxylate (1.01 g) and a 1.5 mol/L solution (6.0 mL) of diisobutylaluminum hydride in toluene, a procedure as in Reference Example 5 was performed to give the title compound as a brown oil (yield 0.84 g, 94%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08048909B2
Source datasetuspto-grants-2011_11
ORD IDord-c6f979b7b802448d96c8d6c577e75ce3
Source noteuspto-grants-2011_11