HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminumhydride → HCID 66924614, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Reactant | HCID 66924727 | HCID 66924727 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 66924614 | HCID 66924614 | 88.1% |
Reaction Steps
Using methyl 4,5-diphenyl-1-(phenylsulfonyl)-1H-pyrrole-3-carboxylate (439 mg) and a 1.5 mol/L solution (3.2 mL) of diisobutylaluminum hydride in toluene, a procedure as in Reference Example 5 was performed to give the title compound as a brown oil (yield 361 mg, 88%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048909B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-50c7b98d88ea47f6a272090e337725cd |
| Source note | uspto-grants-2011_11 |