HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl morpholine oxide → HCID 86232850, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl morpholine oxide | HCID 82029 | — |
| Reactant | HCID 66924627 | HCID 66924627 | — |
| Catalyst | HCID 178419074 | HCID 178419074 | — |
| Product | HCID 86232850 | HCID 86232850 | 101,263.703% |
Reaction Steps
Using [2-methyl-1-(phenylsulfonyl)-5-(3-thienyl)-1H-pyrrol-3-yl]methanol (307 mg), tetra-n-propylammonium perruthenate (26.4 mg), N-methylmorpholine N-oxide (216 mg) and molecular sieves 4A powder (215 mg), a procedure as in Reference Example 6 was performed to give the title compound as a brown oil (yield 309 g, 76%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048909B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-a9549a889f8c45938a1b287bf12d56fe |
| Source note | uspto-grants-2011_11 |