HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl morpholine oxide → HCID 86232858, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl morpholine oxide | HCID 82029 | — |
| Reactant | HCID 66924715 | HCID 66924715 | — |
| Catalyst | HCID 178419074 | HCID 178419074 | — |
| Product | HCID 86232858 | HCID 86232858 | 71% |
Reaction Steps
Using [2,4-dimethyl-5-phenyl-1-(phenylsulfonyl)-1H-pyrrol-3-yl]methanol (0.84 g), tetra-n-propylammonium perruthenate (57.3 mg), N-methylmorpholine N-oxide (437 mg) and molecular sieves 4A powder (422 mg), a procedure as in Reference Example 6 was performed to give the title compound as a brown oil (yield 0.59 g, 71%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048909B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-4baba2b192f44f59873f3aeb6de5d8f3 |
| Source note | uspto-grants-2011_11 |