HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanamine, hydrochloride (1:1) → HCID 66925178, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanamine, hydrochloride (1:1) | HCID 11637 | — |
| Reactant | Sodium cyanoborohydride | HCID 5003444 | — |
| Reactant | HCID 86620773 | HCID 86620773 | — |
| Product | HCID 66925178 | HCID 66925178 | 53.1% |
Reaction Steps
Using 5-(3-methylphenyl)-1-[(4-methylphenyl)sulfonyl]-1H-pyrrole-3-carbaldehyde (0.36 g), methylammonium chloride (0.89 g) and sodium cyanoborohydride (0.21 g), a procedure as in Example 4 was performed to give the title compound as white crystals (yield 0.22 g, 52%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048909B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-6322145a48a34674ad38984a61343f73 |
| Source note | uspto-grants-2011_11 |