HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanamine, hydrochloride (1:1) → HCID 66925163, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanamine, hydrochloride (1:1) | HCID 11637 | — |
| Reactant | Sodium cyanoborohydride | HCID 5003444 | — |
| Reactant | HCID 86620775 | HCID 86620775 | — |
| Product | HCID 66925163 | HCID 66925163 | 80% |
Reaction Steps
Using 5-(2-methylphenyl)-1-[(4-methylphenyl)sulfonyl]-1H-pyrrole-3-carbaldehyde (0.46 g), methylammonium chloride (1.11 g) and sodium cyanoborohydride (0.26 g), a procedure as in Example 4 was performed to give the title compound as colorless crystals (yield 0.37 g, 80%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048909B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-6a569cc779b24669a980d8f48830f9cd |
| Source note | uspto-grants-2011_11 |