HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanamine, hydrochloride (1:1) → HCID 66924883, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanamine, hydrochloride (1:1) | HCID 11637 | — |
| Reactant | Sodium cyanoborohydride | HCID 5003444 | — |
| Reactant | HCID 86620776 | HCID 86620776 | — |
| Product | HCID 66924883 | HCID 66924883 | 72% |
Reaction Steps
Using 5-(4-fluorophenyl)-1-[(4-fluorophenyl)sulfonyl]-1H-pyrrole-3-carbaldehyde (0.52 g), methylammonium chloride (1.20 g) and sodium cyanoborohydride (0.28 g), a procedure as in Example 6 was performed to give the title compound as a colorless oil (yield 0.39 g, 72%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048909B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-74892cc3348848e78a9baac66fb460d3 |
| Source note | uspto-grants-2011_11 |