HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanamine, hydrochloride (1:1) → HCID 66925140, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanamine, hydrochloride (1:1) | HCID 11637 | — |
| Reactant | Sodium cyanoborohydride | HCID 5003444 | — |
| Reactant | HCID 86232862 | HCID 86232862 | — |
| Product | HCID 66925140 | HCID 66925140 | 35.2% |
Reaction Steps
Using 2-methyl-5-phenyl-1-phenylsulfonyl-1H-pyrrole-3-carbaldehyde (0.27 g), methylammonium chloride (0.68 g) and sodium cyanoborohydride (0.28 g), a procedure as in Example 4 was performed to give the title compound as colorless crystals (yield 0.11 g, 35%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048909B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-288a5b7f3b854531aa8d5b1856bde1f3 |
| Source note | uspto-grants-2011_11 |